Background: This study assessed the heavy metal content of selected personal care products (PCPs) used by students of Clifford University, Owerrinta (Ihie Campus), Abia State, Nigeria. The presence of contaminants, particularly heavy metals, in cosmetics is a major concern due to potential health risks. Methods: A total of 24 cosmetic samples, including foundations, face powders, lip glosses, and body creams, were collected from six female hostel rooms. Samples were analyzed for lead (Pb), chromium (Cr), cadmium (Cd), arsenic (As), and mercury (Hg) using atomic absorption spectrophotometry (AAS). Results: Lead concentrations in face powders and lip glosses frequently exceeded Maximum Permissible Limits (MPLs) of 10.00 mg/kg, reaching as high as 20.00 ± 1.01 mg/kg. Mercury in foundations reached 5.73 ± 0.16 mg/kg, far exceeding the 1.00 mg/kg MPL. Cadmium was also above limits in foundation samples. Arsenic and chromium levels generally remained within safe limits. Conclusion: Findings indicate potential health risks due to high levels of toxic metals, particularly lead and mercury. The results highlight a need for stricter regulatory controls and continuous monitoring to safeguard consumer health.